HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-(7-chloro-1-cyclohexyl-1H-indazol-3-yl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 7-chloro-1-cyclohexyl-3-(4-methoxyphenyl)-1H-indazole | HCID 68885462 | — |
| Product | 4-(7-chloro-1-cyclohexyl-1H-indazol-3-yl)phenol | HCID 135525228 | 49.4% |
Reaction Steps
Prepared according to Method C step B from 7-chloro-1-cyclohexyl-3-(4-methoxyphenyl)-1H-indazole (0.55 g, 1.61 mmol), boron tribromide (0.61 mL, 6.5 mmol) and 1.0 mL of cyclohexene to give the product (0.26 g) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-ee80b58397114f5eada78a04fff2c41f |
| Source note | uspto-grants-2007_07 |