HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylhydrazine hydrochloride → 1-cyclohexyl-7-fluoro-3-(4-methoxyphenyl)-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylhydrazine hydrochloride | HCID 207836 | — |
| Reactant | (2,3-Difluorophenyl)(4-methoxyphenyl)methanone | HCID 62650974 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | 1-cyclohexyl-7-fluoro-3-(4-methoxyphenyl)-1H-indazole | HCID 68882127 | 46.2% |
Reaction Steps
Prepared according to Method C step A (2,3-difluorophenyl)-(4-methoxyphenyl)-methanone (0.150 g, 0.6 mmol), cyclohexylhydrazine hydrochloride (0.90 g, 0.6 mmol) and DMAP (0.073 g, 0.6 mmol) to give 0.09 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-20a80a10f17f4e6f84ef830efa4fb41c |
| Source note | uspto-grants-2007_07 |