HRID1294903

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID207836

Cyclohexylhydrazine--hydrogen chloride (1/1)

C6H15ClN2

HCID62650974

(2,3-Difluorophenyl)(4-methoxyphenyl)methanone

C14H10F2O2

PRODUCTS

生成物

结构：COc1ccc(-c2nn(C3CCCCC3)c3c(F)cccc23)cc1

HCID68882127

未命名化合物

收率 46.2%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID14284

N,N-Dimethylpyridin-4-amine

C7H10N2

PROCEDURE

实验过程

Prepared according to Method C step A (2,3-difluorophenyl)-(4-methoxyphenyl)-methanone (0.150 g, 0.6 mmol), cyclohexylhydrazine hydrochloride (0.90 g, 0.6 mmol) and DMAP (0.073 g, 0.6 mmol) to give 0.09 g of the title compound.

WORKUP

后处理

customPrepared