HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopentane → HCID 68882051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopentane | HCID 12335 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178489134 | HCID 178489134 | — |
| Product | HCID 68882051 | HCID 68882051 | 37.5% |
Reaction Steps
Prepared according to Method D step B from 3-(4-methoxyphenyl)-7-trifluoromethyl-1H-indazole (0.146 g, 0.5 mmol), sodium hydride (60% in oil, 0.024 g, 0.6 mmol) and 1-iodopentane (0.130 mL, 1.0 mmol) to give the title compound (0.068 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-3dac0f7c35b043bf922681ef9b9b7eb2 |
| Source note | uspto-grants-2007_07 |