HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-(1-cyclopentyl-7-fluoro-1H-indazol-3-yl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 1-cyclopentyl-7-fluoro-3-(4-methoxyphenyl)-1H-indazole | HCID 68884306 | — |
| Product | 4-(1-cyclopentyl-7-fluoro-1H-indazol-3-yl)phenol | HCID 135524867 | 46.1% |
Reaction Steps
Prepared according to Method D step C from 1-cyclopentyl-7-fluoro-3-(4-methoxyphenyl)-1H-indazole (0.57 g, 1.83 mmol), boron tribromide (0.70 mL, 7.35 mmol) and 3 mL of cyclohexene to give the product (0.25 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-4e52ee9e55e04aa699672878c4e6ac82 |
| Source note | uspto-grants-2007_07 |