HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → 1-cyclopentyl-7-fluoro-3-(4-methoxy-3-methylphenyl)-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178489143 | HCID 178489143 | — |
| Product | 1-cyclopentyl-7-fluoro-3-(4-methoxy-3-methylphenyl)-1H-indazole | HCID 68884760 | 578% |
Reaction Steps
Prepared according to Method D step B from 7-fluoro-3-(4-methoxy-3-methylphenyl)-1H-indazole (0.76 g, 0.4 mmol), sodium hydride (60% in oil, 0.120 g, 3.0 mmol) cyclopentyl bromide (0.321 mL, 3.0 mmol) to give the title compound (0.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-40d10321724c48478154814ebdc76675 |
| Source note | uspto-grants-2007_07 |