HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-[1-(1-Methylethyl)-7-(trifluoromethyl)-1H-indazol-3-yl]-1,3-benzenediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 68883776 | HCID 68883776 | — |
| Product | 4-[1-(1-Methylethyl)-7-(trifluoromethyl)-1H-indazol-3-yl]-1,3-benzenediol | HCID 136355229 | 66.4% |
Reaction Steps
Prepared according to Method D step C from 3-(2,4-dimethoxyphenyl)-1-isopropyl-7-(trifluoromethyl)-1H-indazole (0.442 g, 1.2 mmol), boron tribromide (0.688 mL, 7.27 mmol) and 1.0 mL of cyclohexene to give the product (0.268 g) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f1d295d4a4584af7b2ffbcdd8e5b02a8 |
| Source note | uspto-grants-2007_07 |