HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-[2-allyl-7-(trifluoromethyl)-2H-indazol-3-yl]-3-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 2-allyl-3-(4-methoxy-2-methylphenyl)-7-(trifluoromethyl)-2H-indazole | HCID 68882950 | — |
| Product | 4-[2-allyl-7-(trifluoromethyl)-2H-indazol-3-yl]-3-methylphenol | HCID 135511944 | 80.1% |
Reaction Steps
Prepared according to Method D step C from 2-allyl-3-(4-methoxy-2-methylphenyl)-7-(trifluoromethyl)-2H-indazole (0.043 g, 0.124 mmol), boron tribromide (0.05 mL, 0.52 mmol) and 1.0 mL of cyclohexene to give the product (0.033 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e0608c464de74700b50454a54b3127cd |
| Source note | uspto-grants-2007_07 |