HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopentane → HCID 68884986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopentane | HCID 12335 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178489136 | HCID 178489136 | — |
| Product | HCID 68884986 | HCID 68884986 | 35.9% |
Reaction Steps
Prepared according to Method D step B from 3-(2,4-dimethoxyphenyl)-7-(trifluoromethyl)-1H-indazole (0.150 g, 0.49 mmol), sodium hydride (60% in oil, 0.025 g, 1.04 mmol) and 1-iodopentane (0.07 mL, 0.7 mmol) to give the title compound (0.069 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-24aded73755749a8bb26bccfc7132a9e |
| Source note | uspto-grants-2007_07 |