HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-[1-allyl-7-(trifluoromethyl)-1H-indazol-3-yl]-3-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 1-allyl-3-(4-methoxy-2-methylphenyl)-7-(trifluoromethyl)-1H-indazole | HCID 68883793 | — |
| Product | 4-[1-allyl-7-(trifluoromethyl)-1H-indazol-3-yl]-3-methylphenol | HCID 135524884 | 117.6% |
Reaction Steps
Prepared according to Method D step C from 1-allyl-3-(4-methoxy-2-methylphenyl)-7-(trifluoromethyl)-1H-indazole (0.075 g, 0.22 mmol), boron tribromide (0.082 mL, 0.87 mmol) and 1.0 mL of cyclohexene to give the product (0.086 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-87993599ca7f4026a05d20ccbedf4fb6 |
| Source note | uspto-grants-2007_07 |