HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-(7-fluoro-2-isopropyl-2H-indazol-3-yl)benzene-1,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 3-(2,4-dimethoxyphenyl)-7-fluoro-2-isopropyl-2H-indazole | HCID 68884280 | — |
| Product | 4-(7-fluoro-2-isopropyl-2H-indazol-3-yl)benzene-1,3-diol | HCID 136358462 | 36.5% |
Reaction Steps
Prepared according to Method D step C from 3-(2,4-dimethoxyphenyl)-7-fluoro-2-isopropyl-2H-indazole (0.07 g, 0.22 mmol), boron tribromide (0.12 mL, 1.2 mmol) and 1.0 mL of cyclohexene to give the product (0.023 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-0f028bdef74f4ebdaaa8271887acccbf |
| Source note | uspto-grants-2007_07 |