HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Dimethylaminopyridine → HCID 178489138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 68884772 | HCID 68884772 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178489138 | HCID 178489138 | — |
Reaction Steps
Prepared according to Method D, Step A from (3-chloro-2-fluorophenyl)(3-chloro-4-methoxyphenyl)methanone (2.04 g, 6.82 mmol), hydrazine hydrate (2.5 mL), dimethylaminopyridine (0.97 g) and pyridine (12.5 mL). The title compound was obtained as a white solid and recrystallized from ethyl acetate/hexane (1.74 g, 5.94 mmol, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f08b63ad840f437ba7b5d3d89c456dcd |
| Source note | uspto-grants-2007_07 |