HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetate → HCID 46232857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetate | HCID 84468 | — |
| Reactant | HCID 22063474 | HCID 22063474 | — |
| Reactant | HCID 23105931 | HCID 23105931 | — |
| Product | HCID 46232857 | HCID 46232857 | — |
Reaction Steps
The target compound is obtained by reacting 357 mg (1 mmol) 6-benzyloxy-8-(2-ethoxy-2-hydroxy-acetyl)-4H-benzo[1,4]oxazin-3-one with 233 mg (1 mmol) 1,1-dimethyl-2-(4-trifluoromethoxy-phenyl)-ethylamine using the method described for Example 2c). Beige solid. Yield: 279 mg (50%, trifluoroacetate); mass spectroscopy: [M+H]+=441.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244728B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-7c532280b1ae466c9d1e5ca05426797d |
| Source note | uspto-grants-2007_07 |