HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23105928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 23105941 | HCID 23105941 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23105928 | HCID 23105928 | — |
Reaction Steps
1.50 g (5.9 mmol) 1-(4-chloro-3-trifluoromethyl-phenyl)-2-methyl-propan-1-ol and 0.50 g (2.6 mmol) p-toluenesulphonic acid monohydrate in 50 mL toluene are refluxed for 3 hours using the water separator. After working up analogously to Example 1b) a brown oil is obtained. Yield: 1.4 g; mass spectrometry: [M]+=234/6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244728B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-6658f3f077a344018e7a0c852cfe038c |
| Source note | uspto-grants-2007_07 |