HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetate → HCID 46232973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetate | HCID 84468 | — |
| Reactant | HCID 22063474 | HCID 22063474 | — |
| Reactant | HCID 67133248 | HCID 67133248 | — |
| Product | HCID 46232973 | HCID 46232973 | — |
Reaction Steps
357 mg (1 mmol) 6-benzyloxy-8-(2-ethoxy-2-hydroxy-acetyl)-4H-benzo[1,4]oxazin-3-one and 252 mg (1 mmol) 2-(4-chloro-2-trifluoromethyl-phenyl)-1,1-dimethyl-ethylamine are reacted and worked up analogously to the method described for Example 2c). White solid. Yield: 165 mg (31%, trifluoroacetate); mass spectroscopy [M+H]+=425.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244728B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-1d06af81ac9843609e46612a2d2bf817 |
| Source note | uspto-grants-2007_07 |