HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Amino-2-methylphenol → HCID 10198953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Amino-2-methylphenol | HCID 17818 | — |
| Reactant | HCID 10131256 | HCID 10131256 | — |
| Product | HCID 10198953 | HCID 10198953 | — |
Reaction Steps
Example 11 was prepared as a white solid in 30% overall yield from Compound E using the 2 step sequence of Compound A of Example 1 and Compound B of Example 1, using 3-hydroxy-4-methylaniline. The product was purified by flash chromatography on silica with 25% ethyl acetate/hexanes. (M+H)+ 255.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244733B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-16f9ff3543b34605a1f41963c359223f |
| Source note | uspto-grants-2007_07 |