Hydrochloric Acid → HCID 21843735, compound

Participants

Reaction Steps

9.3 ml of a 2.7M hydrogen chloride solution in diethyl ether are added to 7.2 g (15 mmol) of N-cyclohexylmethyl-2-aminomethyl-8-methoxychroman in 200 ml of diethyl ether at 0° to -10° C., while stirring. After 2 hours, the precipitate is filtered off, washed thoroughly with diethyl ether and dried at 60° C./0.01 mbar.

Provenance & Evidence