HRID1295871
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of (1-benzyl-pyrrolidin-3-ylmethyl)-carbamic acid tert-butyl ester methyl amine (1.0 g, 3.28 mmol) in methanol (35 ml) was added Pd/C (20%) (0.22 g). The resulting mixture was hydrogenated at 50 Psi over night. The Pd was filtered over Celite and evaporated to dryness to give the desired product in 92% yield.
WORKUP
后处理
- filtrationThe Pd was filtered over Celite
- customevaporated to dryness