HRID1295871

反应详情

EQUATION

反应方程式

HRID 1295871 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of (1-benzyl-pyrrolidin-3-ylmethyl)-carbamic acid tert-butyl ester methyl amine (1.0 g, 3.28 mmol) in methanol (35 ml) was added Pd/C (20%) (0.22 g). The resulting mixture was hydrogenated at 50 Psi over night. The Pd was filtered over Celite and evaporated to dryness to give the desired product in 92% yield.

WORKUP

后处理

  1. filtrationThe Pd was filtered over Celite
  2. customevaporated to dryness