Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1295871Generated: October 29, 2026

D-Psicose → HCID 69513333, compound

https://huagongshe.com/reaction/1295871

Reaction equation

Participants

RoleNameHCIDCharge
ReactantD-PsicoseHCID 441036—
ReactantHCID 69513505HCID 69513505—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 69513333HCID 6951333392%

Reaction Steps

To a solution of (1-benzyl-pyrrolidin-3-ylmethyl)-carbamic acid tert-butyl ester methyl amine (1.0 g, 3.28 mmol) in methanol (35 ml) was added Pd/C (20%) (0.22 g). The resulting mixture was hydrogenated at 50 Psi over night. The Pd was filtered over Celite and evaporated to dryness to give the desired product in 92% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07244758B2
Source datasetuspto-grants-2007_07
ORD IDord-a844bc35495b41bbb48f3fdfcfaf5a55
Source noteuspto-grants-2007_07