HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Psicose → HCID 69513333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Psicose | HCID 441036 | — |
| Reactant | HCID 69513505 | HCID 69513505 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69513333 | HCID 69513333 | 92% |
Reaction Steps
To a solution of (1-benzyl-pyrrolidin-3-ylmethyl)-carbamic acid tert-butyl ester methyl amine (1.0 g, 3.28 mmol) in methanol (35 ml) was added Pd/C (20%) (0.22 g). The resulting mixture was hydrogenated at 50 Psi over night. The Pd was filtered over Celite and evaporated to dryness to give the desired product in 92% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244758B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a844bc35495b41bbb48f3fdfcfaf5a55 |
| Source note | uspto-grants-2007_07 |