HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22929889, compound → HCID 22929650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22929889 | HCID 22929889 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22929650 | HCID 22929650 | — |
Reaction Steps
After dissolving tert-butyl 4-(azidomethyl)-5-cyano-2-ethoxybenzoate (1.923 g) in dichloromethane (12 ml), trifluoroacetic acid (3 ml) was added while cooling on ice. The mixture was stirred at room temperature for 20 minutes and concentrated. The title compound was obtained as light red crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244730B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-bdea8125bf704f8a93b3d585594e51a5 |
| Source note | uspto-grants-2007_07 |