HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzyl Alcohol → HCID 16641047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzyl Alcohol | HCID 125 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | p-Trifluoromethylbenzyl chloride | HCID 123096 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16641047 | HCID 16641047 | — |
Reaction Steps
4-Hydroxymethyl-phenol (1 g, 8.06 mmol), 1-Chloromethyl-4-trifluoromethyl-benzene (1.57 g, 8.06 mmol), and cesium carbonate (5.26 g, 16.12 mmol) were refluxed in acetonitrile for 20 h, cooled, filtered, and concentrated to give the title compound. MS m/z 265 (M−H2O+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244763B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-310c376259344908ab9161dd7e368a59 |
| Source note | uspto-grants-2007_07 |