Hydrochloric Acid → HCID 11737031, compound

Participants

Reaction Steps

To (±)-N-(t-butoxycarbonyl)-1,3,4,10b-tetrahydro-7-chloropyrazino[2,1-a]isoindol-6(2H)-one (15 mg, 0.05 mmol) was added concentrated hydrochloric acid (1 mL). After 15 min, the resulting solution was concentrated, diluted with water, and lyopholized to give (±)-1,3,4,10b-tetrahydro-7-chloro-pyrazino[2,1-a]isoindol-6(2H)-one hydrochloric acid salt as an off-white solid (12 mg, 100%). MS (ESI) 223.2, 225.2 (M−Cl).

Provenance & Evidence