HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178443434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178526951 | HCID 178526951 | — |
| Solvent | 1-Decanol | HCID 8174 | — |
| Product | HCID 178443434 | HCID 178443434 | — |
Reaction Steps
A solution of 2.5 g (8.4 mmol) of 6-[2-(1H-Tetrazol-5-yl)-ethyl]-decahydro-isoquinoline-3-carboxylic acid monohydrate in 50 ml decyl alcohol saturated with hydrogen chloride (g) is heated at 120° C. overnight. The mixture is concentrated in vacuo and the residue purified by SPE (Oasis HLB) to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247644B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-55361ea9e1a14da2a3d3920cabc41564 |
| Source note | uspto-grants-2007_07 |