Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21063702 | HCID 21063702 | — |
| Product | HCID 19372152 | HCID 19372152 | — |
Reaction Steps
0.37 cm3 of thionyl chloride are added to 23 cm3 of methanol cooled to -20° C. and 980 mg of 17-aminoheptadecanoic acid are added. The solution is stirred for 12 hours at a temperature in the region of 20° C. and the solvent is removed under reduced pressure (2.7 kPa) at a temperature in the region of 40° C. 1.08 g of methyl 17-aminoheptadecanoate hydrochloride are thus obtained in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05468888 |
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| Source dataset | uspto-grants-1995_11 |
|---|
| ORD ID | ord-59e3ea71b3dd4ed2bb6e4b8a81529280 |
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| Source note | uspto-grants-1995_11 |
|---|
