Sodium hydride → HCID 18186809, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure of example 4, step 1 starting from 2,6-dichloropyrazine (298 mg, 2.00 mmol), 2-methoxybenzyl alcohol (303 mg, 2.20 mmol) and NaH (55% in mineral oil, 96 mg, 2.2 mmol). The yield of the crude product was 0.49 g (98%) and was used directly as such in the next step. MS m/z 250 (M)+. HRMS m/z calcd for C12H11ClN2O2 (M)+ 250.0509, found 250.0522.

Provenance & Evidence