HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18186916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,6-Dichloropyrazine | HCID 78504 | — |
| Reactant | 1-Benzyl-3-ethylpiperazine | HCID 22036541 | — |
| Product | HCID 18186916 | HCID 18186916 | — |
Reaction Steps
The title compound was prepared according to the procedure of example 39, step 2, starting from the product obtained in step 1 above (4.60 g, 22.5 mmol), 2,6-dichloropyrazine (3.90 g, 26.2 mmol) and K2CO3 (6.22 g, 45.0 mmol). Yield: 6.15 g (86%). MS m/z 316/318 (M)+ (35Cl/37Cl-isotope pattern). HRMS m/z calcd for C17H21ClN4 (M)+ 316.1455, found 316.1455.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247633B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-123083806e1244809b7871dc5c6e47ea |
| Source note | uspto-grants-2007_07 |