HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenethyl alcohol → HCID 18186896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenethyl alcohol | HCID 69705 | — |
| Reactant | 2,6-Dichloropyrazine | HCID 78504 | — |
| Product | HCID 18186896 | HCID 18186896 | — |
Reaction Steps
The title compound was prepared according to the procedure of example 50, step 1, starting from 4-methoxyphenethyl alcohol (1.99 g, 13.1 mmol), K-t-BuO (1.34 g, 12.0 mmol) and 2,6-dichloropyrazine (1.56 g, 10.5 mmol). The yield of the title compound was 2.14 g (77%) and was obtained as a white solid. Anal. (C13H13ClN2O2) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247633B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-94f009ef37b344b48c0ec1e7fef05333 |
| Source note | uspto-grants-2007_07 |