HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → HCID 18186864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | 1-Hexanol | HCID 8103 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18186938 | HCID 18186938 | — |
| Product | HCID 18186864 | HCID 18186864 | — |
Reaction Steps
The title compound was prepared according to the procedure of example 50, step 2, starting from 2-chloro-6-(n-hexyloxy)pyrazine (1.54 g, 7.17 mmol; obtained according to the procedure of example 50, step 1, starting from n-hexanol), piperazine (1.90 g, 22.1 mmol) and K2CO3 (0.99 g, 7.16 mmol). The yield of the title compound was 1.21 g (64%) which was obtained as a colorless oil. HRMS m/z calcd for C14H24N4O (M)+ 264.1950, found 264.1953. Anal. (C14H24N4O) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247633B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a07b58d8830747e3930e97bad0095e51 |
| Source note | uspto-grants-2007_07 |