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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296677Generated: October 30, 2026

Piperazine → HCID 18186864, compound

https://huagongshe.com/reaction/1296677

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPiperazineHCID 4837—
Reactant1-HexanolHCID 8103—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 18186938HCID 18186938—
ProductHCID 18186864HCID 18186864—

Reaction Steps

The title compound was prepared according to the procedure of example 50, step 2, starting from 2-chloro-6-(n-hexyloxy)pyrazine (1.54 g, 7.17 mmol; obtained according to the procedure of example 50, step 1, starting from n-hexanol), piperazine (1.90 g, 22.1 mmol) and K2CO3 (0.99 g, 7.16 mmol). The yield of the title compound was 1.21 g (64%) which was obtained as a colorless oil. HRMS m/z calcd for C14H24N4O (M)+ 264.1950, found 264.1953. Anal. (C14H24N4O) C, H, N.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247633B2
Source datasetuspto-grants-2007_07
ORD IDord-a07b58d8830747e3930e97bad0095e51
Source noteuspto-grants-2007_07