HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 10286478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 6-Quinoxalinamine | HCID 237859 | — |
| Reactant | 1-Azabicyclo[2.2.2]octane-3-carbonyl chloride | HCID 11446616 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 10286478 | HCID 10286478 | — |
Reaction Steps
In analogy to the method described in Example 2, 250 mg (2.57 mmol) of 3-quinuclidinecarbonyl chloride, 461 mg (3.57 mmol) of N,N-diisopropylethylamine, catalytic amounts of DMAP (approx. 1 mg) and 173 mg (1.19 mmol) of 6-quinoxalinylamine are reacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247728B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e7b98ee681594d558f71bd129c002042 |
| Source note | uspto-grants-2007_07 |