HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 178518194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | (R)-2-Amino-2-(4-fluorophenyl)ethanol | HCID 10583003 | — |
| Reactant | HCID 178503545 | HCID 178503545 | — |
| Product | HCID 178518194 | HCID 178518194 | — |
Reaction Steps
Then similar procedure as described in example 14b was used, starting from 2-methylsulfanyl-5-(1H-pyrrolo[2,3-b]pyridin-3-ylmethylene)-thiazol-4-one (example 14a), 2-[(R)-1-(4-fluoro-phenyl)-2-hydroxy-ethylamine and DIEA to give 2-[(R)-1-(4-fluoro-phenyl)-2-hydroxy-ethylamino]-5-[1-(1H-pyrrolo[2,3-b]pyridin-3-yl)-meth-(Z)-ylidene]-thiazol-4-one. LC-MS m/e 383 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247727B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-591383c500d14f9f996d2f55e20a7364 |
| Source note | uspto-grants-2007_07 |