HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → [4-(4-Ethylpiperazin-1-yl)phenyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 4-(4-ethylpiperazin-1-yl)benzaldehyde | HCID 10513024 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | [4-(4-Ethylpiperazin-1-yl)phenyl]methanol | HCID 23514389 | — |
Reaction Steps
This compound was prepared in the manner of Step A, Example 5, using 0.4 gram (0.019 mole) of [4-(4-ethylpiperazinyl)benzaldehyde and 0.4 gram (0.01 mole) of sodium borohydride in 40 mL of absolute ethanol (available from J. T. Baker Inc.) The yield of the title compound was 0.3 gram. The NMR Spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247756B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-814abed4cdbf46feb4e3a1da0b1f7214 |
| Source note | uspto-grants-2007_07 |