HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 58913640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 58913651 | HCID 58913651 | — |
| Product | HCID 58913640 | HCID 58913640 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 2-(4-Bromo-phenyl)-1-(5-chloro-2,4-dihydroxy-phenyl)-ethanone (1.5 g, 4.4 mmol), Acetic anhydride (2.0 ml), Potassium carbonate (2.1 g 15.2 mmol). 3-(4-Bromo-phenyl)-6-chloro-7-hydroxy-2-methyl-chromen-4-one was obtained an off white solid (1.2 g, 74.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-af45297177b242908863cf2422ffb449 |
| Source note | uspto-grants-2007_07 |