HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-(2-Bromo-phenyl)-6-chloro-7-hydroxy-2-methyl-chromen-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2-Bromo-phenyl)-1-(5-chloro-2,4-dihydroxy-phenyl)-ethanone | HCID 58913586 | — |
| Product | 3-(2-Bromo-phenyl)-6-chloro-7-hydroxy-2-methyl-chromen-4-one | HCID 58913501 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 2-(2-Bromo-phenyl)-1-(5-chloro-2,4-dihydroxy-phenyl)-ethanone (2.0 g, 5.88 mmol), acetic anhydride (2.0 ml), potassium carbonate (2.5 g 18.1 mmol). The white precipitate formed was shown to contain the required compound and was taken directly onto the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e23d6ceb7ed64c8cae07c048eda1ab52 |
| Source note | uspto-grants-2007_07 |