HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | (3'-Ethoxy-biphenyl-4-yl)-acetic acid | HCID 2758741 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 58913671 | HCID 58913671 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.26 g, 1.8 mmol), (3′-Ethoxybiphenyl-4-yl)-acetic acid (0.44 g, 1.8 mmol), BF3Et2O (5 ml), PCl5 (0.56 g, 2.69 mmol), DMF (8 ml and 5 ml). The crude oil product (0.39 g, 55.2%) was taken onto the next stage. Rf 0.8 ethyl acetate/hexane (70/30)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-c9aff849d4a742f0afe6e67ef5964e6a |
| Source note | uspto-grants-2007_07 |