HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 22225974 | HCID 22225974 | — |
| Product | HCID 58913645 | HCID 58913645 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.15 g, 1.0 mmol), (3′,4′-dimethoxy-biphenyl-3-yl)-acetic acid (0.28 g, 1 mmol), BF3Et2O (5 ml), PCl5 (0.32 g, 1.5 mmol), DMF (6 ml and 4 ml). The white precipitate formed was shown to contain the required compound and was taken directly onto the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-9fb7ee51c9c44b5a9c64d59d8d97354b |
| Source note | uspto-grants-2007_07 |