HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2-Methoxyphenylacetic acid | HCID 7134 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Product | HCID 58913587 | HCID 58913587 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (1.74 g, 12.0 mmol), 2-methoxyphenylacetic acid (2.0 g, 12.0 mmol), BF3Et2O (10 ml), PCl5 (3.76 g, 18.1 mmol), DMF (20 ml and 10 ml). The pale brown solid precipitate was taken directly onto the next stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-c87310f3a2124578ae00ff562c387848 |
| Source note | uspto-grants-2007_07 |