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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296889Generated: October 30, 2026

4-Chlororesorcinol → HCID 58913639, compound

https://huagongshe.com/reaction/1296889

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-ChlororesorcinolHCID 1731—
ReactantDimethylformamideHCID 6228—
ReactantPhosphorus pentachlorideHCID 24819—
ReactantHCID 58913654HCID 58913654—
ProductHCID 58913639HCID 58913639—

Reaction Steps

This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.33 g, 2.28 mmol), [3-(3-Cyano-propoxy)-phenyl]-acetic acid (0.5 g, 2.28 mmol), BF3Et2O (5 ml), PCl5 (0.71 g, 3.4 mmol), DMF (8 ml and 5 ml). Crude 4-[3-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-butyronitrile was obtained as an oil which was taken onto the next stage without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247734B2
Source datasetuspto-grants-2007_07
ORD IDord-4e1c98c06e964944be5701a154866be2
Source noteuspto-grants-2007_07