HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 58913654 | HCID 58913654 | — |
| Product | HCID 58913639 | HCID 58913639 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.33 g, 2.28 mmol), [3-(3-Cyano-propoxy)-phenyl]-acetic acid (0.5 g, 2.28 mmol), BF3Et2O (5 ml), PCl5 (0.71 g, 3.4 mmol), DMF (8 ml and 5 ml). Crude 4-[3-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-butyronitrile was obtained as an oil which was taken onto the next stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-4e1c98c06e964944be5701a154866be2 |
| Source note | uspto-grants-2007_07 |