HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 58913596 | HCID 58913596 | — |
| Product | HCID 58913665 | HCID 58913665 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.125 g, 0.87 mmol), [2-(3-Cyano-propoxy)-phenyl]-acetic acid (0.19 g, 0.87 mmol), BF3Et2O (5 ml), PCl5 (0.27 g, 1.3 mmol), DMF (8 ml and 5 ml). Crude 4-[2-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-butyronitrile was obtained as an oil which was taken onto the next stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-1b45ffa6f1014e32bd2def959c3f812d |
| Source note | uspto-grants-2007_07 |