Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296890Generated: November 2, 2026

4-Chlororesorcinol → HCID 58913665, compound

https://huagongshe.com/reaction/1296890

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-ChlororesorcinolHCID 1731—
ReactantDimethylformamideHCID 6228—
ReactantPhosphorus pentachlorideHCID 24819—
ReactantHCID 58913596HCID 58913596—
ProductHCID 58913665HCID 58913665—

Reaction Steps

This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (0.125 g, 0.87 mmol), [2-(3-Cyano-propoxy)-phenyl]-acetic acid (0.19 g, 0.87 mmol), BF3Et2O (5 ml), PCl5 (0.27 g, 1.3 mmol), DMF (8 ml and 5 ml). Crude 4-[2-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-butyronitrile was obtained as an oil which was taken onto the next stage without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247734B2
Source datasetuspto-grants-2007_07
ORD IDord-1b45ffa6f1014e32bd2def959c3f812d
Source noteuspto-grants-2007_07