HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Benzeneacetic acid, 2-fluoro- | HCID 67979 | — |
| Product | HCID 58913663 | HCID 58913663 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (1.889, 13.0 mmol), 2-fluorophenylacetic acid (2.0 g, 13 mmol), BF3Et2O (10 ml), PCl5 (4.0 g, 19.2 mmol), DMF (20 ml and 10 ml). The pale white precipitate formed was shown to contain the required compound and was taken directly onto the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-10240e50173b4d62bed02d7168401a77 |
| Source note | uspto-grants-2007_07 |