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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296896Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 178515921, compound

https://huagongshe.com/reaction/1296896

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
Reactant3-(4-bromophenyl)-7-hydroxy-4H-chromen-4-oneHCID 5398367—
SolventEthanolHCID 702—
ProductHCID 178515921HCID 178515921—

Reaction Steps

This compounds was synthesised in the same manner as described in the preceding experiment. 3-(4-Bromo-phenyl)-7-hydroxy-chromen-4-one (0.1 g, 0.3 mmol), hydrazine hydrate (4 ml), ethanol (10 ml). The crude solid product was washed in hot ether to give 4-[4-(4-Bromo-phenyl)-1H-pyrazol-3-yl]-benzene-1,3-diol as a white solid (0.069, 60.6%); Rf 0.44 Cf SM 0.79 ethyl acetate/hexane (75/25).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247734B2
Source datasetuspto-grants-2007_07
ORD IDord-6cea44d539ca4d548c3c6b40f49a33af
Source noteuspto-grants-2007_07