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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296898Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 178435604, compound

https://huagongshe.com/reaction/1296898

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
Reactant6-Ethyl-7-hydroxy-3-phenyl-chromen-4-oneHCID 5399651—
SolventEthanolHCID 702—
ProductHCID 178435604HCID 178435604—

Reaction Steps

This compounds was synthesised in the same manner as described above. 6-Ethyl-7-hydroxy-3-phenyl-chromen-4-one (0.29 g, 1.1 mmol), hydrazine hydrate (4 ml), ethanol (20 ml). The crude product was columned to give 4-Ethyl-6-(4-phenyl-1H-pyrazol-3-yl)-benzene-1,3-diol as a off white solid (0.23 g, 74.73%); Rf 0.7 Cf SM 0.9 ethyl acetate/hexane (70/30).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247734B2
Source datasetuspto-grants-2007_07
ORD IDord-1d4679dcdfe0406cad8c4454bcf1f803
Source noteuspto-grants-2007_07