HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178435604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 6-Ethyl-7-hydroxy-3-phenyl-chromen-4-one | HCID 5399651 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178435604 | HCID 178435604 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 6-Ethyl-7-hydroxy-3-phenyl-chromen-4-one (0.29 g, 1.1 mmol), hydrazine hydrate (4 ml), ethanol (20 ml). The crude product was columned to give 4-Ethyl-6-(4-phenyl-1H-pyrazol-3-yl)-benzene-1,3-diol as a off white solid (0.23 g, 74.73%); Rf 0.7 Cf SM 0.9 ethyl acetate/hexane (70/30).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-1d4679dcdfe0406cad8c4454bcf1f803 |
| Source note | uspto-grants-2007_07 |