HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178511014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 58913601 | HCID 58913601 | — |
| Product | HCID 178511014 | HCID 178511014 | 87% |
Reaction Steps
This compound was synthesised in the same manner as described above. 5-[3-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-pentanenitrile (0.1 g, 0.27 mmol), Hydrazine hydrate (5 ml). The precipitate formed on quenching was filtered to give 5-{3-[3-(5-Chloro-2,4-dihydroxy-phenyl)-1H-pyrazol-4-yl]-phenoxy}-pentanenitrile as a white solid (0.09 g, 87.0%); Rf 0.6 ethyl acetate/hexane (70/30)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-c536cd0af04440308f55737ca0ee6bb8 |
| Source note | uspto-grants-2007_07 |