HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinoethanol → HCID 136049264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinoethanol | HCID 8017 | — |
| Reactant | HCID 58913628 | HCID 58913628 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136049264 | HCID 136049264 | — |
Reaction Steps
3-(4-Bromo-phenyl)-6-chloro-7-hydroxy-chromen-4-one (0.1 g, 0.28 mmol), and 2-Hydrazino-ethanol (0.04 g) were suspended in ethanol (10 ml) and refluxed for 1 hr. 4-[4-(4-Bromo-phenyl)-1-(2-hydroxy-ethyl)-1H-pyrazol-3-yl]-6-chloro-benzene-1,3-diol precipitated out on quenching as a white solid (0.09 g, 78.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-08388c1358994e889113a42429edb6b8 |
| Source note | uspto-grants-2007_07 |