HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 4,4-Diphenylbutan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1,1-Diphenylbutane-1,4-diol | HCID 96679 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4,4-Diphenylbutan-1-ol | HCID 92519 | — |
Reaction Steps
11.2 g (46.2 mmol) of 1,1-diphenyl-1,4-butanediol was hydrogenated (45° C., 5 atm) in 100 ml of methanol in the presence of 0.5 ml of concentrated sulfuric acid and 10% palladium/carbon to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247645B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-d373cd1919ee4ec7b8ad42622650291c |
| Source note | uspto-grants-2007_07 |