HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 15575966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 53725716 | HCID 53725716 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 15575966 | HCID 15575966 | — |
Reaction Steps
10 ml of methanol was added to a mixture of 320 mg (1.34 mmol) of 5,5-diphenyl-2-pentene-1-ol and a catalytic amount of 10% palladium/carbon, and they were stirred in hydrogen atmosphere at room temperature under ambient pressure for 12 hours. The catalyst was filtered out and the obtained filtrate was concentrated under reduced pressure to obtain the unpurified title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247645B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-46b8a7bd2e8c482c8bb8ae20720f8a9c |
| Source note | uspto-grants-2007_07 |