HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Diphenylpropanol → (3,3-Diphenylpropane-1-yl)4-chloroacetoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Diphenylpropanol | HCID 29908 | — |
| Reactant | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | (3,3-Diphenylpropane-1-yl)4-chloroacetoacetate | HCID 86760519 | — |
Reaction Steps
3.2 ml (23.7 mmol) of ethyl 4-chloroacetoacetate and 5.00 g (23.6 mmol) of 3,3-diphenyl-1-propanol were heated at 130° C. in 100 ml of toluene overnight. Toluene was distilled out under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247645B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e835d43cf5de477aaacabebde4532375 |
| Source note | uspto-grants-2007_07 |