HRID1297028

反应详情

EQUATION

反应方程式

HRID 1297028 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3.2 ml (23.7 mmol) of ethyl 4-chloroacetoacetate and 5.00 g (23.6 mmol) of 3,3-diphenyl-1-propanol were heated at 130° C. in 100 ml of toluene overnight. Toluene was distilled out under reduced pressure to obtain the title compound.

WORKUP

后处理

  1. distillationToluene was distilled out under reduced pressure