HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 69427723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 3-Chlorobenzaldehyde | HCID 11477 | — |
| Reactant | 2-Cyanoethyl 3-oxobutanoate | HCID 12360406 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 69427723 | HCID 69427723 | — |
Reaction Steps
1.00 g (6.45 mmol) of 2-cyanoethyl acetoacetate and 730 μl (6.44 mmol) of 3-chlorobenzaldehyde were stirred in the presence of a catalytic amount of acetic acid and piperidine in 100 ml of 2-propanol at room temperature overnight. The solvent was evaporated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247645B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-be115c3215564dbc99bbe588d9f59e94 |
| Source note | uspto-grants-2007_07 |