Piperidine → HCID 86586137, compound

Participants

Reaction Steps

1.12 g (5.00 mmol) of 3-(2-cyanoethoxycarbonyl)benzaldehyde, 1.38 g (5.03 mmol) of 1-(4-benzyl[1,4]-diazepane-1-yl)butane-1,3-dion and 0.05 ml (0.51 mmol) of piperidine were stirred in 50 ml of benzene at 105° C. overnight. Ethyl acetate was added to the reaction mixture. After drying over anhydrous sodium sulfate, the product was concentrated under reduced pressure to obtain the title compound.

Provenance & Evidence