HRID129725

反应详情

EQUATION

反应方程式

HRID 129725 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Quinoline-3-carbaldehyde (1.57 g) and 1.21 g of L-cysteine were dissolved in 50 ml of 50% ethanol, and the solution was stirred at room temperature for 1 hour. The resultant crystalline precipitate was collected by suction filtrating, washed with 50% ethanol and dried to give 1.95 g of 2-(3-quinolyl)thiazolidine-4-carboxylic acid. Melting point 173°-175° C. (decomposition).

WORKUP

后处理

  1. customThe resultant crystalline precipitate was collected by suction
  2. filtrationfiltrating
  3. washwashed with 50% ethanol
  4. customdried